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Incomplete conversion of hemiacetals 1ad to HCHO under acidic DNPH conditions is observed, leading to underestimation of their levels as HCHO equivalents When solutions enriched in 1a d were applied to standard DNPH solutions or DNPH sorbent tubes, 33% of the hemiacetals were not detected (i.e., not converted to HCHO) using the DNPH impinger method, and 46% were not detected via the DNPH sorbent tube method

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